(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

Base Information

Chemical Name:(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride
CAS No.:740800-74-2
Molecular Formula:C₂₈H₂₂Cl₂N₄O₄
Molecular Weight:549.413
Hs Code.:

(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[<i>g</i>]cyclopenta[<i>cd</i>]azulen-2-yl)-acetyl chloride

Synonyms:(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

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Chemical Property of (3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

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Technology Process of (3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

There total 5 articles about (3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 740800-73-1
(3-carboxymethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetic acid

: 740800-74-2
(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.tetlet.2004.05.040

Reference yield:

: 740800-71-9
2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

: 740800-74-2
(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butoxide / dimethylsulfoxide / 0.5 h

1.2: 46 percent / dimethylsulfoxide / 6 h

2.1: 84 percent / lithium hydroxide; methanol / 20 °C

3.1: 100 percent / oxalyl chloride; DMF / CH₂Cl₂

With methanol; lithium hydroxide; oxalyl dichloride; potassium tert-butylate; N,N-dimethyl-formamide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2004.05.040

Reference yield:

: 740800-72-0
(3-methoxycarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetic acid methyl ester

: 740800-74-2
(3-chlorocarbonylmethyl-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-yl)-acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / lithium hydroxide; methanol / 20 °C

2: 100 percent / oxalyl chloride; DMF / CH₂Cl₂

With methanol; lithium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.tetlet.2004.05.040