3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

Base Information

Chemical Name:3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one
CAS No.:649551-82-6
Molecular Formula:C₄₁H₄₆O₆
Molecular Weight:634.813
Hs Code.:

Synonyms:3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

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Chemical Property of 3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

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Technology Process of 3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

There total 9 articles about 3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 124186-79-4
(rac)-1-iodo-3,7-dimethyloctane

: 649551-78-0
3-benzyloxy-7-iodo-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-chromen-4-one

: 649551-82-6
3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

Guidance literature:: (rac)-1-iodo-3,7-dimethyloctane; With magnesium; zinc(II) chloride; In tetrahydrofuran; at 50 ℃; for 20h;

3-benzyloxy-7-iodo-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-chromen-4-one; With dichlorobis(tri-O-tolylphosphine)palladium; In tetrahydrofuran; for 25h;
DOI:10.1016/j.bmc.2004.02.031

Reference yield:

: 106-24-1
Geraniol

: 649551-82-6
3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: 55 percent / H₂ / Pd/C / ethanol / 21 h

2.1: 71 percent / iodine; triphenylphosphine; imidazole / toluene / 18 h

3.1: magnesium; zinc chloride / tetrahydrofuran / 20 h / 50 °C

3.2: 30 percent / dichlorobis[tri(o-tolyl)phosphine]palladium / tetrahydrofuran / 25 h

With 1H-imidazole; hydrogen; iodine; magnesium; triphenylphosphine; zinc(II) chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; toluene; 3.2: Negishi cross-coupling;
DOI:10.1016/j.bmc.2004.02.031

Reference yield:

: 106-21-8,59204-02-3
tetrahydrogeraniol

: 649551-82-6
3-benzyloxy-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-7-(3,7-dimethyl-octyl)-chromen-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 71 percent / iodine; triphenylphosphine; imidazole / toluene / 18 h

2.1: magnesium; zinc chloride / tetrahydrofuran / 20 h / 50 °C

2.2: 30 percent / dichlorobis[tri(o-tolyl)phosphine]palladium / tetrahydrofuran / 25 h

With 1H-imidazole; iodine; magnesium; triphenylphosphine; zinc(II) chloride; In tetrahydrofuran; toluene; 2.2: Negishi cross-coupling;
DOI:10.1016/j.bmc.2004.02.031