(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

Base Information

Chemical Name:(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside
CAS No.:1063630-40-9
Molecular Formula:C₃₉H₄₄O₇
Molecular Weight:624.774
Hs Code.:

Synonyms:(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

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Technology Process of (3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

There total 1 articles about (3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1063630-38-5
5-(3,4,5-tris(benzyloxy)-6-benzyloxymethyl-tetrahydropyran-2-yl)pent-2-en-1-ol

: 1063630-40-9
(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate; In dichloromethane; toluene; at -20 ℃; for 18h;
DOI:10.1016/j.tet.2008.06.007

Reference yield: 64.0%

: 1063630-40-9
(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

: 1063630-68-1
(3'R,4'S)-1-C-(3'-azido-4',5'-dihydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

Guidance literature:: With titanium(IV) isopropylate; trimethylsilylazide; In benzene; at 80 ℃;
DOI:10.1016/j.tet.2008.06.007

Reference yield:

: 1063630-40-9
(3'R,4'R)-1-C-(3',4'-epoxy-5'-hydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

: 1063630-44-3
C₃₉H₄₅N₃O₇

: 1063630-42-1
(3'S,4'S)-1-C-(3'-azido-4',5'-dihydroxypentyl)-2,3,4,6-tetra-O-benzyl-α-D-galactopyranoside

Guidance literature:: With sodium azide; ammonium chloride; In methanol; water; at 80 ℃; for 16h; Title compound not separated from byproducts.;
DOI:10.1016/j.tet.2008.06.007