C₃₇H₄₆N₂O₈S

Base Information

Chemical Name:C₃₇H₄₆N₂O₈S
CAS No.:1408065-17-7
Molecular Formula:C₃₇H₄₆N₂O₈S
Molecular Weight:678.847
Hs Code.:

C<sub>37</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₃₇H₄₆N₂O₈S

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Chemical Property of C₃₇H₄₆N₂O₈S

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Technology Process of C₃₇H₄₆N₂O₈S

There total 8 articles about C₃₇H₄₆N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1408065-16-6
C₂₂H₃₆N₂O₆S

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1408065-17-7
C₃₇H₄₆N₂O₈S

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 17h; Inert atmosphere;
DOI:10.1039/c2ob26103k

Reference yield:

: 5978-22-3,1426213-63-9
N(ε)-benzoyloxycarbonyl-L-lysine tert-butyl ester hydrochloride

: 1408065-17-7
C₃₇H₄₆N₂O₈S

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; sodium cyanoborohydride / methanol / 2 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: 10% Pd/C; hydrogen / ethyl acetate / 13 h / 20 °C / 760.05 Torr

4: potassium carbonate / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

With 10% Pd/C; hydrogen; sodium cyanoborohydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c2ob26103k

Reference yield:

: (4-iodophenyl)-acetic acid benzyl ester

: 1408065-17-7
C₃₇H₄₆N₂O₈S

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / toluene / 18 h / Inert atmosphere; Reflux

2: trichloroisocyanuric acid; benzyltrimethylammonium chloride / acetonitrile / 0.28 h / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

4: 10% Pd/C; hydrogen / ethyl acetate / 13 h / 20 °C / 760.05 Torr

5: potassium carbonate / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

With copper(l) iodide; trichloroisocyanuric acid; 10% Pd/C; hydrogen; benzyltrimethylammonium chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; acetonitrile;
DOI:10.1039/c2ob26103k