3-benzyl-5-pgebylsulfonylmethylisoxazoline

Base Information

• Chemical Name: 3-benzyl-5-pgebylsulfonylmethylisoxazoline
• CAS No.: 244176-62-3
• Molecular Formula: C₁₇H₁₇NO₃S
• Molecular Weight: 315.393
• Mol file: 244176-62-3.mol

Synonyms:3-benzyl-5-pgebylsulfonylmethylisoxazoline

Chemical Property of 3-benzyl-5-pgebylsulfonylmethylisoxazoline

Chemical Property:

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Technology Process of 3-benzyl-5-pgebylsulfonylmethylisoxazoline

There total 1 articles about 3-benzyl-5-pgebylsulfonylmethylisoxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(allylsulfonyl)benzene (16212-05-8) + Phenylacetaldehyde oxime (7028-48-0) → 3-benzyl-5-pgebylsulfonylmethylisoxazoline (244176-62-3)

Guidance literature:

With pyridine; sodium hypochlorite; In chloroform; at 0 ℃; for 2h;

DOI:10.1080/00397919908085941

Reference yield: 99.0%

3-benzyl-5-pgebylsulfonylmethylisoxazoline (244176-62-3) → 1-phenyl-pent-4-en-2-one oxime

Guidance literature:

With magnesium; mercury dichloride; In methanol; at -23 ℃; for 1.5h;

DOI:10.1080/00397919908085941

Reference yield: 98.0%

3-benzyl-5-pgebylsulfonylmethylisoxazoline (244176-62-3) → (E)-1-phenyl-3-penten-2-one oxime (244176-69-0)

Guidance literature:

With magnesium; mercury dichloride; In methanol; at 0 - 20 ℃; for 6h;

DOI:10.1080/00397919908085941

upstream raw materials:

(allylsulfonyl)benzene

Phenylacetaldehyde oxime

Downstream raw materials:

(E)-1-phenyl-3-penten-2-one oxime

(E)-1-phenyl-3-penten-2-one