3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

Base Information

Chemical Name:3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one
CAS No.:502633-60-5
Molecular Formula:C₂₂H₂₇NO₃SSe
Molecular Weight:464.487
Hs Code.:

Synonyms:3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

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Chemical Property of 3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

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Technology Process of 3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

There total 7 articles about 3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1666-13-3
diphenyl diselenide

: 502633-52-5
2,2-dimethylpent-4-enoic acid hydroxy[2-(toluene-4-sulfonyl)ethyl]amide

: 502633-60-5
3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

Guidance literature:: With diethyl phosphorylchloridite; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -50 - 20 ℃; for 2h;

Reference yield:

: 16386-93-9
2,2-dimethylpent-4-enoic acid

: 502633-60-5
3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2; DMF / CH₂Cl₂ / 1.25 h / 0 - 20 °C

2: Et₃N / CH₂Cl₂ / 2.25 h / 0 - 20 °C

3: 78 percent / DIEA; (EtO)2PCl / CH₂Cl₂ / 2 h / -50 - 20 °C

With diethyl phosphorylchloridite; oxalyl dichloride; triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 39482-46-7
2,2-dimethylpent-4-enoyl chloride

: 502633-60-5
3,3-dimethyl-5-phenylselanylmethyl-1-[2-(toluene-4-sulfonyl)ethyl]pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 2.25 h / 0 - 20 °C

2: 78 percent / DIEA; (EtO)2PCl / CH₂Cl₂ / 2 h / -50 - 20 °C

With diethyl phosphorylchloridite; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;