1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

Base Information

Chemical Name:1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one
CAS No.:1276024-98-6
Molecular Formula:C₂₂H₂₂N₄O₂
Molecular Weight:374.442
Hs Code.:

Synonyms:1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

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Chemical Property of 1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

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Technology Process of 1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

There total 6 articles about 1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276025-02-5
C₂₄H₂₆N₄O₃

: 1276024-98-6
1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

Guidance literature:: C₂₄H₂₆N₄O₃; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3.5h;

With sodium hydrogencarbonate; In water;

Reference yield:

: 149507-27-7
4-(4-cyanophenyl)cyclohexanone-ethylene ketal

: 1276024-98-6
1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 3.5 h / -40 - 20 °C

1.2: 0 °C

2.1: acetic acid / 1.67 h

3.1: hydrogen; acetic acid / palladium 10% on activated carbon / 20 h / 4137.29 Torr

4.1: triethylamine / tetrahydrofuran / 18.5 h / Reflux

5.1: trifluoroacetic acid / dichloromethane / 3.5 h / 0 - 20 °C

With hydrogen; diisobutylaluminium hydride; acetic acid; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1276024-99-7
C₁₅H₁₈O₃

: 1276024-98-6
1-(1H-benzo[d]imidazol-5-yl)-5-(4-(4-oxocyclohexyl)phenyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 1.67 h

2: hydrogen; acetic acid / palladium 10% on activated carbon / 20 h / 4137.29 Torr

3: triethylamine / tetrahydrofuran / 18.5 h / Reflux

4: trifluoroacetic acid / dichloromethane / 3.5 h / 0 - 20 °C

With hydrogen; acetic acid; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane;