2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

Base Information

Chemical Name:2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical
CAS No.:198570-86-4
Molecular Formula:C₁₃H₁₅FN₃O₄
Molecular Weight:296.278
Hs Code.:

Synonyms:2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

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Chemical Property of 2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

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Technology Process of 2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

There total 4 articles about 2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 53104-28-2
2-(4′-fluorophenyl)-4,4,5,5-tetramethyl-imidazoline-1-oxyl-3-oxide

: 198570-86-4
2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

Guidance literature:: With sulfuric acid; nitric acid; at 0 - 20 ℃; for 0.5h;
DOI:10.1055/s-1997-1311

Reference yield:

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 198570-86-4
2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / aq. Na₂CO₃ / methanol / 40 h / Ambient temperature

2: 55 percent / PbO₂ / CHCl₃

3: 62 percent / H₂SO₄, HNO₃ / 0.5 h / 0 - 20 °C

With sulfuric acid; nitric acid; sodium carbonate; lead dioxide; In methanol; chloroform;
DOI:10.1055/s-1997-1311

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 198570-86-4
2-(4-fluoro-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-yl-oxyl 3-oxide radical

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / aq. Na₂CO₃ / methanol / 40 h / Ambient temperature

2: 55 percent / PbO₂ / CHCl₃

3: 62 percent / H₂SO₄, HNO₃ / 0.5 h / 0 - 20 °C

With sulfuric acid; nitric acid; sodium carbonate; lead dioxide; In methanol; chloroform;
DOI:10.1055/s-1997-1311