2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

Base Information

Chemical Name:2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide
CAS No.:1432912-67-8
Molecular Formula:C₉H₆F₃N₃O₂S₂
Molecular Weight:309.293
Hs Code.:

Synonyms:2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

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Chemical Property of 2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

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Technology Process of 2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

There total 2 articles about 2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 220227-21-4
2,4,5-trifluorobenzene-1-sulfonyl chloride

: 100703-97-7
N-methyl-1,2,4-thiadiazol-5-amine

: 1432912-67-8
2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

Guidance literature:: N-methyl-1,2,4-thiadiazol-5-amine; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

2,4,5-trifluorobenzene-1-sulfonyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

Reference yield: 27.0%

: 220227-21-4
2,4,5-trifluorobenzene-1-sulfonyl chloride

: N-methyl-1,2,4-thiadiazol-5-amine hydrochloride

: 1432912-67-8
2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

Guidance literature:: N-methyl-1,2,4-thiadiazol-5-amine hydrochloride; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

2,4,5-trifluorobenzene-1-sulfonyl chloride; In tetrahydrofuran; at -78 - 20 ℃;

Reference yield: 63.0%

: 1432912-60-1
2-(2-amino-1H-benzo[d]imidazol-5-yl)-4-chlorophenol

: 1432912-67-8
2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

: 1432913-40-0
GX-4197

Guidance literature:: 2-(2-amino-1H-benzo[d]imidazol-5-yl)-4-chlorophenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h;

2,4,5-trifluoro-N-methyl-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 16h;