C₁₄H₁₆BNO₂

Base Information

• Chemical Name: C₁₄H₁₆BNO₂
• CAS No.: 1268936-26-0
• Molecular Formula: C₁₄H₁₆BNO₂
• Molecular Weight: 241.098
• Mol file: 1268936-26-0.mol

Synonyms:C₁₄H₁₆BNO₂

Chemical Property of C₁₄H₁₆BNO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₄H₁₆BNO₂

There total 1 articles about C₁₄H₁₆BNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

N,N-dimethyl O-(quinolyl-6) carbamate (115580-96-6) + 2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane (201733-56-4) → C14H16BNO2 (1268936-26-0)

Guidance literature:

With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride; In 1,2-dimethoxyethane; toluene; at 120 ℃; for 48h; Inert atmosphere;

DOI:10.1002/chem.201001943

Reference yield: 80.0%

C14H16BNO2 (1268936-26-0) + (1H-pyrrol-1-yl)(3,4,5-trimethoxyphenyl)methanone → 1-(3,4,5-trimethoxyphenyl)-1-(quinolin-6-yl)methanone (1215208-59-5)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; 1,1'-((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(3-(2,6-diisopropylphenyl)-1H-imidazol-3-ium) chloride; In water; toluene; at 80 ℃; for 20h; Inert atmosphere; Sealed tube; Darkness;

DOI:10.1039/c7cc07457c

Reference yield: 70.0%

N-benzoylpyrrole (5145-65-3) + C14H16BNO2 (1268936-26-0) → phenyl(quinolin-6-yl)methanone (54885-02-8)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; 1,1'-((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(3-(2,6-diisopropylphenyl)-1H-imidazol-3-ium) chloride; In water; toluene; at 80 ℃; for 20h; Inert atmosphere; Sealed tube; Darkness;

DOI:10.1039/c7cc07457c

upstream raw materials:

N,N-dimethyl O-(quinolyl-6) carbamate

2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

Downstream raw materials:

phenyl(quinolin-6-yl)methanone

1-(3,4,5-trimethoxyphenyl)-1-(quinolin-6-yl)methanone

Refernces