IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Base Information

Chemical Name:IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)
CAS No.:103746-18-5
Molecular Formula:C₃₆H₆₃ClIrP₃
Molecular Weight:816.49
Hs Code.:

IrH<sub>2</sub>Cl(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>11</sub>)2)2)

Synonyms:IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Suppliers and Price of IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

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Technology Process of IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

There total 2 articles about IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 145036-82-4
IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

: 103746-18-5
IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Guidance literature:: With hydrogen; In benzene; nitrogen atmosphere; a soln. of the Ir complex (prepared in situ) is stirred for 0.5 h; hydrogen bubbled into the reaction mixt. (2 h); removal of the solvent in vac.; residue dissolved in THF; treatment with abs. ethanol; solid collected and dried in vac.; elem. anal.;

Reference yield: 40.0%

: chloro(1,5-cyclooctadiene)iridium(I) dimer

: 70786-89-9
Cyttp

: 103746-18-5
IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Guidance literature:: In ethanol; benzene; nitrogen atmosphere; a benzene soln. of the ligand is added to a soln. of the Ir complex in abs. EtOH; refluxing (2 h), removal of the solvent (vac.), residue dissolved in CH2Cl2, addn. of ethanol; removal of most of the CH2Cl2 under reduced pressure; solid collected, washed (ether), and dried in vac.; elem. anal.;

Reference yield: 81.0%

: 103746-18-5
IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

: 145036-97-1
IrHCl₂(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; nitrogen atmosphere; aq. HCl added to the soln. of the Ir complex, mixt. stirred for 3 h; solvent removal (red. pressure), washing (hexanes); elem. anal.;