C₁₀H₁₄O

Base Information

Chemical Name:C₁₀H₁₄O
CAS No.:1448446-12-5
Molecular Formula:C₁₀H₁₄O
Molecular Weight:150.221
Hs Code.:

Synonyms:C₁₀H₁₄O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₄O

Chemical Property:

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Technology Process of C₁₀H₁₄O

There total 5 articles about C₁₀H₁₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₉H₁₄O₂

: 18107-18-1
diazomethyl-trimethyl-silane

: 1448446-12-5
C₁₀H₁₄O

Guidance literature:: diazomethyl-trimethyl-silane; With n-butyllithium; diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; at -78 - -50 ℃; for 0.333333h; Inert atmosphere;

C₉H₁₄O₂; In tetrahydrofuran; diethyl ether; hexane; at -78 - 25 ℃; Inert atmosphere;
DOI:10.1002/anie.201209300

Reference yield:

: 138124-05-7
(1S,6R)-(-)-8-Oxabicyclo<4.3.0>non-2-en-7-one

: 1448446-12-5
C₁₀H₁₄O

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

3.1: n-butyllithium; diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

3.2: -78 - 25 °C / Inert atmosphere

With n-butyllithium; diisobutylaluminium hydride; diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201209300

Reference yield:

: 4949-20-6,52192-01-5
2,4-pentadien-1-ol

: 1448446-12-5
C₁₀H₁₄O

Guidance literature:: Multi-step reaction with 4 steps

1.1: (R)-1,1'-Bi-2-naphthol; dimethyl zinc(II); methylmagnesium bromide / dichloromethane; toluene; diethyl ether / 0.17 h / 80 °C / Inert atmosphere

1.2: 0 - 25 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

4.1: n-butyllithium; diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

4.2: -78 - 25 °C / Inert atmosphere

With n-butyllithium; methylmagnesium bromide; dimethyl zinc(II); (R)-1,1'-Bi-2-naphthol; diisobutylaluminium hydride; diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; 1.2: |Diels-Alder Cycloaddition / 2.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201209300