Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Base Information

Chemical Name:Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester
CAS No.:117120-85-1
Molecular Formula:C₁₆H₂₀N₄O₄S
Molecular Weight:364.425
Hs Code.:

Synonyms:Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

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Chemical Property of Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

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Technology Process of Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

There total 3 articles about Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 624-83-9
methyl isocyanate

: 117121-02-5
1-phenyl-2-(methylthio)-4,5-bis (hydroxymethyl)imidazole

: 117120-85-1
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 144h; Heating;
DOI:10.1021/jm00121a023

Reference yield:

: 117121-07-0
diethyl 2-mercapto-1-phenylimidazole-4,5-dicarboxylate

: 117120-85-1
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaOCH₃

2: 81 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

3: 82 percent / triethylamine / CH₂Cl₂ / 144 h / Heating

With lithium aluminium tetrahydride; sodium methylate; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm00121a023

Reference yield:

: 117120-96-4
dimethyl 2-(methylthio)-1-phenylimidazole-4,5-dicarboxylate

: 117120-85-1
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-2-methylsulfanyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

2: 82 percent / triethylamine / CH₂Cl₂ / 144 h / Heating

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm00121a023