2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

Base Information

Chemical Name:2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid
CAS No.:1038821-41-8
Molecular Formula:C₁₈H₂₃Cl₂NO₇
Molecular Weight:436.289
Hs Code.:

Synonyms:2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

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Chemical Property of 2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

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Technology Process of 2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

There total 1 articles about 2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1038821-39-4
2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannitol

: 1038821-41-8
2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

Guidance literature:: With sodium hypochlorite; tetrabutyl-ammonium chloride; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In sodium hydrogencarbonate; at 0 - 25 ℃; for 2h;
DOI:10.1016/j.bmc.2008.03.045

Reference yield: 30.0%

: 1038821-41-8
2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

: 99-09-2
3-nitro-aniline

: 1038821-46-3
N-(3-nitrophenyl)-2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 20h;
DOI:10.1016/j.bmc.2008.03.045

Reference yield: 29.0%

: 1038821-41-8
2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonic acid

: 107-11-9,30551-89-4
1-amino-2-propene

: 1038821-45-2
N-allyl-2,5-anhydro-1-deoxy-1-[(tert-butoxycarbonyl)(3,4-dichlorobenzyl)amino]-D-mannonamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 20h;
DOI:10.1016/j.bmc.2008.03.045