{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

Base Information

Chemical Name:{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol
CAS No.:255827-68-0
Molecular Formula:C₅₈H₉₄O₇
Molecular Weight:903.38
Hs Code.:

Synonyms:{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

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Chemical Property of {4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

Chemical Property:

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Technology Process of {4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

There total 6 articles about {4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 255827-67-9
{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-benzyloxy}-tert-butyl-diphenyl-silane

: 255827-68-0
{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 20h;
DOI:10.1002/(SICI)1521-3765(19991105)5:11<3221::AID-CHEM3221>3.0.CO;2-P

Reference yield:

: 111-83-1
1-bromo-octane

: 255827-68-0
{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / K₂CO₃; 18-crown-6 / acetone / 60 h / Heating

2.1: LiAlH₄ / diethyl ether / 4 h / Heating

3.1: PPh₃; CBr₄ / tetrahydrofuran / 20.75 h / 0 - 20 °C

4.1: NaH / tetrahydrofuran / 1 h / 20 °C

4.2: 99 percent / tetrahydrofuran / 18 h / 20 - 66 °C

5.1: TBAF / tetrahydrofuran / 20 h

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; diethyl ether; acetone; 1.1: Etherification / 2.1: Reduction / 3.1: Substitution / 4.1: Metallation / 4.2: Etherification / 5.1: Desilylation;
DOI:10.1002/(SICI)1521-3765(19991105)5:11<3221::AID-CHEM3221>3.0.CO;2-P

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 255827-68-0
{4-[(2S,3R)-3-(3,5-Bis-octyloxy-benzyloxy)-2-(3,5-bis-octyloxy-benzyloxymethyl)-butyl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / K₂CO₃; 18-crown-6 / acetone / 60 h / Heating

2.1: LiAlH₄ / diethyl ether / 4 h / Heating

3.1: PPh₃; CBr₄ / tetrahydrofuran / 20.75 h / 0 - 20 °C

4.1: NaH / tetrahydrofuran / 1 h / 20 °C

4.2: 99 percent / tetrahydrofuran / 18 h / 20 - 66 °C

5.1: TBAF / tetrahydrofuran / 20 h

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; diethyl ether; acetone; 1.1: Etherification / 2.1: Reduction / 3.1: Substitution / 4.1: Metallation / 4.2: Etherification / 5.1: Desilylation;
DOI:10.1002/(SICI)1521-3765(19991105)5:11<3221::AID-CHEM3221>3.0.CO;2-P