(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide

Base Information

• Chemical Name: (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide
• CAS No.: 960060-68-8
• Molecular Formula: C₂₂H₂₄F₃NO₃
• Molecular Weight: 407.433

Synonyms:(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide

Chemical Property of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide

Chemical Property:

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Technology Process of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide

There total 2 articles about (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C22H24F3NO3 (960060-54-2) → (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide (960060-68-8)

Guidance literature:

With di-μ-chlorobis[η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-1'H-imidazolyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadienyl)-iron(II)]dipalladium(II); silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 50 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.200900712

Reference yield:

2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-ethyl-5-benzyloxypent-2-enyl ester → (S)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethylallyl)acetamidate + (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-ethyl-1-allyl)acetamide (960060-68-8)

Guidance literature:

With silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; ferrocenyl 1-Ts-2,3-Ph₂-imidazoline palladacycle catalyst; In dichloromethane; at 50 ℃; for 60h; Title compound not separated from byproducts.;

DOI:10.1002/anie.200702086

upstream raw materials:

C₂₂H₂₄F₃NO₃

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