1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

Base Information

Chemical Name:1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide
CAS No.:1416065-68-3
Molecular Formula:C₂₃H₂₄N₃*I
Molecular Weight:469.368
Hs Code.:

Synonyms:1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

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Chemical Property of 1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

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Technology Process of 1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

There total 4 articles about 1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1416065-67-2
2-(N-phenylamino)-3-(N-isopropylamino)-6-(2',6'-dimethylphenyl)pyridine

: 122-51-0
orthoformic acid triethyl ester

: 1416065-68-3
1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

Guidance literature:: With ammonium iodide; for 18h; Reflux;

Reference yield:

: 62476-56-6
3-amino-2,6-dichloropyridine

: 1416065-68-3
1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: borane dimethyl sulfide complex / dichloromethane; acetic acid / 3 h / 0 - 20 °C

2: sodium t-butanolate; (±)-2,2'-bis(diphenyl-phosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 24 h / Reflux

3: sodium hydroxide / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 1,4-dioxane; water / 18 h / Reflux

4: ammonium iodide / 18 h / Reflux

With ammonium iodide; (±)-2,2'-bis(diphenyl-phosphino)-1,1'-binaphthyl; borane dimethyl sulfide complex; sodium hydroxide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; acetic acid; toluene;

Reference yield:

: 1416065-63-8
2,6-dichloro-3-(N-isopropylamino)pyridine

: 1416065-68-3
1-isopropyl-3-phenyl-5-(2',6'-dimethylphenyl)-4-azabenzimidazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium t-butanolate; (±)-2,2'-bis(diphenyl-phosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 24 h / Reflux

2: sodium hydroxide / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 1,4-dioxane; water / 18 h / Reflux

3: ammonium iodide / 18 h / Reflux

With ammonium iodide; (±)-2,2'-bis(diphenyl-phosphino)-1,1'-binaphthyl; sodium hydroxide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In 1,4-dioxane; water; toluene;