(1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one

Base Information

• Chemical Name: (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one
• CAS No.: 97321-82-9
• Molecular Formula: C₂₁H₂₀O₅
• Molecular Weight: 352.387

Synonyms:(1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one

Chemical Property of (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one

There total 4 articles about (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.8%

(1SR,2SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.03,8>tridecan-2-ol (97321-80-7,97372-25-3,97373-05-2) → (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.03,8>tridecan-2-one (97321-82-9)

Guidance literature:

With sodium periodate; ruthenium tetroxide; sodium hydrogencarbonate; In chloroform; water; at 0 - 5 ℃; for 7.5h;

DOI:10.1016/0008-6215(85)85187-9

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) → (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.03,8>tridecan-2-one (97321-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 25.4 percent / toluene-p-sulfonic acid monohydrate / dimethylformamide / 8.5 h / 55 °C

2: 64.8 percent / sodium hydrogencarbonate, sodium metaperiodate, ruthenium tetraoxide / CHCl₃; H₂O / 7.5 h / 0 - 5 °C

With sodium periodate; ruthenium tetroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; In chloroform; water; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(85)85187-9

Reference yield:

DL-(1,2/3,4,5)-5-hydroxymethyl-1,2,3,4-cyclohexanetetrol (10226-73-0,16656-62-5,16802-98-5,52079-85-3,64625-68-9,74560-71-7,74561-03-8,74561-07-2,74561-10-7,86117-80-8,86117-81-9,86117-82-0,90694-07-8,94943-08-5,94943-09-6,95043-48-4,96647-89-1,97372-13-9,97372-19-5,97372-28-6,97372-30-0,102629-13-0,105017-74-1,105017-81-0,108867-09-0,109668-67-9,135820-00-7) → (1SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.03,8>tridecan-2-one (97321-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 25.4 percent / toluene-p-sulfonic acid monohydrate / dimethylformamide / 8.5 h / 55 °C

2: 64.8 percent / sodium hydrogencarbonate, sodium metaperiodate, ruthenium tetraoxide / CHCl₃; H₂O / 7.5 h / 0 - 5 °C

With sodium periodate; ruthenium tetroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; In chloroform; water; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(85)85187-9

upstream raw materials:

(1SR,2SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-ol

benzaldehyde dimethyl acetal

DL-(1,2/3,4,5)-5-hydroxymethyl-1,2,3,4-cyclohexanetetrol

DL-(1,2/3,4,5)-5-acethoxymethyl-1,2,3,4-tetra-O-acetyl-1,2,3,4-cyclohexanetetrol

Downstream raw materials:

(1SR,2RS,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-ol

(1SR,2SR,3SR,5SR,8RS,10SR,12RS)-5,12-diphenyl-4,6,11,13-tetraoxatricyclo<8.3.0.0^3,8>tridecan-2-ol

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