3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

Base Information

Chemical Name:3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide
CAS No.:84669-87-4
Molecular Formula:C₁₃H₁₆N₂OS
Molecular Weight:248.349
Hs Code.:

Synonyms:3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

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Technology Process of 3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

There total 6 articles about 3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 84670-00-8
N-benzyl-N'-(3-chloro-2,2-dimethylpropionyl)thiourea

: 84669-87-4
3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

Guidance literature:: With sodium hydroxide; phase transfer catalist; In dichloromethane; Ambient temperature;
DOI:10.1246/cl.1982.1791

Reference yield: 53.0%

: 4300-97-4
3-Chloropivaloyl chloride

: 621-83-0
N-benzylthiourea

: 84669-87-4
3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1246/cl.1982.1791

Reference yield: 33.0%

: 4300-97-4
3-Chloropivaloyl chloride

: 621-83-0
N-benzylthiourea

: 84669-87-4
3,3-Dimethyl-2-oxo-azetidine-1-carbothioic acid benzylamide

: 99121-82-1
3-(3-Benzyl-thioureido)-2,2-dimethyl-propionic acid

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; for 12h; Ambient temperature;