Technology Process of (C5H5)2Ti(SCH2CH2P(C6H5)2CH3)2(2+)*2I(1-)=(C5H5)2Ti(SCH2CH2P(C6H5)2CH3I)2
There total 1 articles about (C5H5)2Ti(SCH2CH2P(C6H5)2CH3)2(2+)*2I(1-)=(C5H5)2Ti(SCH2CH2P(C6H5)2CH3I)2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methyl iodide;
In
tetrahydrofuran;
under N2, 3 equiv of CH3I was added dropwise with stirring to 1 equiv of Ti-complex in freshly distd. degassed THF, stirred for 2 h; concd., volume reduiced, filtered, washed with THF; elem. anal.;