C₁₆H₂₀O₃

Base Information

Chemical Name:C₁₆H₂₀O₃
CAS No.:1332721-92-2
Molecular Formula:C₁₆H₂₀O₃
Molecular Weight:260.333
Hs Code.:

C<sub>16</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:C₁₆H₂₀O₃

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Chemical Property of C₁₆H₂₀O₃

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Technology Process of C₁₆H₂₀O₃

There total 1 articles about C₁₆H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955959-44-1
((2R,6R)-7-benzyloxy)-2,6-dimethylhept-3-yn-1-ol

: 1332721-92-2
C₁₆H₂₀O₃

Guidance literature:: With Jones reagent; In acetone; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol202306d

Reference yield:

: 1332721-92-2
C₁₆H₂₀O₃

: C₁₆H₁₉ClO₂

Guidance literature:: With thionyl chloride; In toluene; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ol202306d

Reference yield:

: 1332721-92-2
C₁₆H₂₀O₃

: 955959-48-5
(3R,3aS,4S,6aS)-4-((R)-3-(benzyloxy)-2-methylpropyl)-dihydro-3a-hydroxy-6a-(hydroxymethyl)-1,3-dimethyl-1H-furo[3,4-b]pyrrole-2,6(3H,6aH)-dione

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / toluene / 10 h / 0 - 20 °C / Inert atmosphere

2.1: toluene / 2 h / 0 - 20 °C / Inert atmosphere

3.1: indium(III) triflate; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 6 h / Inert atmosphere; Reflux

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 41 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 25 h / 20 °C / Inert atmosphere

6.2: 0.5 h / -78 °C / Inert atmosphere

With indium(III) triflate; osmium(VIII) oxide; thionyl chloride; oxalyl dichloride; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol202306d