(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

Base Information

Chemical Name:(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate
CAS No.:295803-73-5
Molecular Formula:C₁₉H₂₀N₂O₇
Molecular Weight:388.377
Hs Code.:

Synonyms:(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

Chemical Property:

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Technology Process of (S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

There total 2 articles about (S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109278-11-7
(S)-(+)-methyl 2-benzoylamino-3-(3,4-dimethoxyphenyl)propanoate

: 295803-73-5
(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

Guidance literature:: With nitric acid; In chloroform; at 0 ℃; for 6h;
DOI:10.1016/S0040-4020(00)00470-1

Reference yield:

: methyl 2-benzoylamino-3-(3,4-dimethoxyphenyl)-2-propenoate

: 295803-73-5
(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.67 g / H₂ / [(COD)Rh-(1,2-bis((2S,5S)-dimethylphospholano)benzene)]OTf / methanol / 6 h / 20 °C / 1810.02 Torr

2: fuming nitric acid / CHCl₃ / 6 h / 0 °C

With hydrogen; nitric acid; (+)-1,2-bis-((2S,5S)-2,5-diethylphospholano)benzene(cyclooctadiene)rhodium(I) trifluoromethanesulfonate; In methanol; chloroform; 1: Catalytic hydrogenation / 2: Nitration;
DOI:10.1016/S0040-4020(00)00470-1

Reference yield:

: 295803-73-5
(S)-(-)-methyl 2-benzoylamino-3-(3,4-dimethoxy-6-nitrophenyl)propanoate

: 295803-74-6
(S)-(+)-3-benzoylamino-6,7-dimethoxy-1,2,3,4-tetrahydro-2-oxoquinoline

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; acetic acid; for 18h; under 2585.74 Torr;
DOI:10.1016/S0040-4020(00)00470-1