9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Base Information

Chemical Name:9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione
CAS No.:1246366-65-3
Molecular Formula:C₂₉H₃₁N₃O₄
Molecular Weight:485.583
Hs Code.:

Synonyms:9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

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Chemical Property of 9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

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Technology Process of 9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

There total 2 articles about 9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 329734-82-9
2-[(4,4-dimethyl-2,6-dioxocyclohexyl)-(4-nitrophenyl)methyl]-5,5-dimethylcyclohexane-1,3-dione

: 95-54-5
1,2-diamino-benzene

: 1246366-65-3
9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: In acetic acid; for 12h; Reflux;
DOI:10.1016/j.tetlet.2010.06.041

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1246366-65-3
9-(4-nitrophenyl)-3,3,6,6,-tetramethyl-10-(2-aminophenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; water / Heating

2: acetic acid / Reflux

With acetic acid; In methanol; water;
DOI:10.1016/j.jphotochem.2010.10.025