N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

Base Information

Chemical Name:N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide
CAS No.:138963-17-4
Molecular Formula:C₄₁H₄₄N₂O₇S
Molecular Weight:708.876
Hs Code.:

Synonyms:N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

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Technology Process of N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

There total 2 articles about N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 138963-17-4
N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

Guidance literature:: With acetic acid; In toluene; for 1.5h; Heating;
DOI:10.1002/hlca.19910740845

Reference yield:

: 139212-74-1,140851-31-6
N-sodio-N'-(2,3,4,6-tetra-O-benzyl-D-glucopyranosylidene)-4-toluenesulfonohydrazidate

: 138963-17-4
N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 12 percent / phenol / tetrahydrofuran / 5 h / Irradiation

2: 82 percent / AcOH / toluene / 1.5 h / Heating

With acetic acid; phenol; In tetrahydrofuran; toluene;
DOI:10.1002/hlca.19910740845

Reference yield: 81.0%

: 138963-17-4
N'-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-4-toluenesulfonohydrazide

: 138963-18-5
N'-(2,3,4,6-tetra-O-benzyl-D-glucopyranosylidene)-4-toluenesulfonohydrazide

Guidance literature:: With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; for 0.75h; Ambient temperature;
DOI:10.1002/hlca.19910740845