(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

Base Information

Chemical Name:(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane
CAS No.:154140-32-6
Molecular Formula:C₁₆H₂₃IO₂
Molecular Weight:374.262
Hs Code.:

Synonyms:(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

Chemical Property:

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Technology Process of (2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

There total 4 articles about (2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Toluene-4-sulfonic acid (2R,3R)-3-((1R,3S)-3-benzyloxy-1-methyl-butyl)-2-methyl-oxiranylmethyl ester

: 154140-32-6
(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

Guidance literature:: With sodium iodide; In acetone; for 3h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)61604-0

Reference yield:

: 154140-31-5
[(2R,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-methyl-oxiranyl]-methanol

: 154140-32-6
(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / diethyl ether / 0.5 h / 0 °C

2: NaI / acetone / 3 h / Ambient temperature

With potassium hydroxide; sodium iodide; In diethyl ether; acetone;
DOI:10.1016/S0040-4039(00)61604-0

Reference yield:

: (E)-(4R,6S)-6-Benzyloxy-2,4-dimethyl-hept-2-en-1-ol

: 154140-32-6
(2S,3R)-3-((1R,3S)-3-Benzyloxy-1-methyl-butyl)-2-iodomethyl-2-methyl-oxirane

Guidance literature:: Multi-step reaction with 3 steps

1: MCPBA / CH₂Cl₂ / 2 h / 0 °C

2: KOH / diethyl ether / 0.5 h / 0 °C

3: NaI / acetone / 3 h / Ambient temperature

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)61604-0