C₄₉H₇₄Cl₃N₅O₁₄

Base Information

Chemical Name:C₄₉H₇₄Cl₃N₅O₁₄
CAS No.:226067-32-9
Molecular Formula:C₄₉H₇₄Cl₃N₅O₁₄
Molecular Weight:1063.51
Hs Code.:

C<sub>49</sub>H<sub>74</sub>Cl<sub>3</sub>N<sub>5</sub>O<sub>14</sub>

Synonyms:C₄₉H₇₄Cl₃N₅O₁₄

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Chemical Property of C₄₉H₇₄Cl₃N₅O₁₄

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Technology Process of C₄₉H₇₄Cl₃N₅O₁₄

There total 25 articles about C₄₉H₇₄Cl₃N₅O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35793-73-8
N-(tert-butyloxycarbonyl)-γ-benzyl-D-glutamic acid

: 226067-32-9
C₄₉H₇₄Cl₃N₅O₁₄

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / diethyl ether / 0 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 1.5 h

3: 601 mg / BOP; DIPEA / CH₂Cl₂ / 44 h / 20 °C

4: TFA / CH₂Cl₂

5: 153 mg / HATU; collidine / dimethylformamide; CH₂Cl₂; toluene / 16 h / 0 - 20 °C

With 2,3,5-trimethyl-pyridine; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja0206700

Reference yield:

: 194149-69-4
(E)-(4S, 5S)-methyl-4-azido-6-hydroxy-5-methyl-hex-2-enoate

: 226067-32-9
C₄₉H₇₄Cl₃N₅O₁₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: imidazole / dimethylformamide / 6 h / 0 - 20 °C

2.1: SnCl₂; MeOH / 6 h / 0 - 20 °C

3.1: aq. NaHCO₃ / dioxane / 24 h / 20 °C

4.1: O₃; pyridine / methanol / -78 °C

4.2: Me₂S / methanol / 7 h / -78 - 20 °C

5.1: 973 mg / CrCl₂ / tetrahydrofuran / 5 h / 20 °C

6.1: Cp₂Zr(H)Cl / tetrahydrofuran / 1 h / 50 °C

6.2: ZnCl₂ / tetrahydrofuran / 0.03 h / 20 °C

6.3: 81 percent / Pd(PPh₃)4 / tetrahydrofuran / 0.33 h / 20 °C

7.1: 95 percent / TBAF*SiO₂ / tetrahydrofuran / 4 h / 20 °C

8.1: 87 percent / TPAP; NMO; H₂O / acetonitrile / 18 h / 20 °C

9.1: 153 mg / HATU; collidine / dimethylformamide; CH₂Cl₂; toluene / 16 h / 0 - 20 °C

With pyridine; 1H-imidazole; chromium dichloride; 2,3,5-trimethyl-pyridine; methanol; Schwartz's reagent; N-methyl-2-indolinone; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; water; silica gel; sodium hydrogencarbonate; ozone; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; tin(ll) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 5.1: Takai homologation;
DOI:10.1021/ja0206700

Reference yield:

: 474085-58-0
(E)-(4S,5S)-4-Amino-6-(tert-butyl-diphenyl-silanyloxy)-5-methyl-hex-2-enoic acid methyl ester

: 226067-32-9
C₄₉H₇₄Cl₃N₅O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: aq. NaHCO₃ / dioxane / 24 h / 20 °C

2.1: O₃; pyridine / methanol / -78 °C

2.2: Me₂S / methanol / 7 h / -78 - 20 °C

3.1: 973 mg / CrCl₂ / tetrahydrofuran / 5 h / 20 °C

4.1: Cp₂Zr(H)Cl / tetrahydrofuran / 1 h / 50 °C

4.2: ZnCl₂ / tetrahydrofuran / 0.03 h / 20 °C

4.3: 81 percent / Pd(PPh₃)4 / tetrahydrofuran / 0.33 h / 20 °C

5.1: 95 percent / TBAF*SiO₂ / tetrahydrofuran / 4 h / 20 °C

6.1: 87 percent / TPAP; NMO; H₂O / acetonitrile / 18 h / 20 °C

7.1: 153 mg / HATU; collidine / dimethylformamide; CH₂Cl₂; toluene / 16 h / 0 - 20 °C

With pyridine; chromium dichloride; 2,3,5-trimethyl-pyridine; Schwartz's reagent; N-methyl-2-indolinone; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; water; silica gel; sodium hydrogencarbonate; ozone; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Takai homologation;
DOI:10.1021/ja0206700