Technology Process of 2,5-diphenyl-3-propylfuran
There total 3 articles about 2,5-diphenyl-3-propylfuran which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine; dipotassium peroxodisulfate; fac-Ir(2-phenylpyridine)3;
In
dimethyl sulfoxide;
at 20 ℃;
for 24h;
Inert atmosphere;
Irradiation;
DOI:10.1002/chem.201602053
- Guidance literature:
-
With
triphenylphosphine;
bis(dibenzylideneacetone)-palladium(0);
In
toluene;
at 70 ℃;
for 6h;
DOI:10.1055/s-1987-28157
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-chloro-succinimide; toluene-4-sulfonic acid / 80 °C
2: fac-Ir(2-phenylpyridine)3; dipotassium peroxodisulfate; 2,6-dimethylpyridine / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere; Irradiation
With
2,6-dimethylpyridine; dipotassium peroxodisulfate; N-chloro-succinimide; fac-Ir(2-phenylpyridine)3; toluene-4-sulfonic acid;
In
dimethyl sulfoxide;
DOI:10.1002/chem.201602053
