2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

Base Information

Chemical Name:2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine
CAS No.:1011465-97-6
Molecular Formula:C₂₀H₃₂N₂O₅
Molecular Weight:380.484
Hs Code.:

Synonyms:2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

Chemical Property:

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Technology Process of 2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

There total 4 articles about 2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1011466-22-0
C₁₅H₂₄N₂O₃

: 24424-99-5
di-tert-butyl dicarbonate

: 1011465-97-6
2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2013.12.085

Reference yield:

: 83197-70-0
(S)-2-(benzyloxycarbonylamino)propyl methanesulfonate

: 1011465-97-6
2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / Reflux

2: triethylamine / dichloromethane / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2013.12.085

Reference yield:

: 6429-44-3,61425-27-2,87905-97-3,66674-16-6
(S)-(-)-N-(benzyloxycarbonyl)alaninol

: 1011465-97-6
2-(S)-2-(benzyloxycarbonyl)amino-N-(tert-butoxycarbonyl)-N-(4-hydroxybutyl)propylamine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 20 °C

2: tetrahydrofuran / Reflux

3: triethylamine / dichloromethane / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2013.12.085