C₂₃H₃₆O₄

Base Information

Chemical Name:C₂₃H₃₆O₄
CAS No.:1412947-74-0
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

C<sub>23</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₂₃H₃₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₆O₄

Chemical Property:

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Technology Process of C₂₃H₃₆O₄

There total 7 articles about C₂₃H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1412947-63-7
C₂₃H₃₄O₂

: 1412947-74-0
C₂₃H₃₆O₄

Guidance literature:: With AD-mix β; water; In tert-butyl alcohol; at 0 - 5 ℃;
DOI:10.1039/c2cc36260k

Reference yield:

: 88920-24-5
p-methoxybenzyloxy acetic acid

: 1412947-74-0
C₂₃H₃₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

4.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium iodide / butanone / 24 h / Reflux

6.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

6.2: 0 - 20 °C

7.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; water; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; dichloromethane; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k

Reference yield:

: 65733-27-9
cis-piperitol

: 1412947-74-0
C₂₃H₃₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

4.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium iodide / butanone / 24 h / Reflux

6.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

6.2: 0 - 20 °C

7.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; water; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; dichloromethane; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k