phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester

Base Information

• Chemical Name: phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester
• CAS No.: 1261073-47-5
• Molecular Formula: C₁₃H₁₃N₃OS
• Molecular Weight: 259.332
• Mol file: 1261073-47-5.mol

Synonyms:phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester

Chemical Property of phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester

Chemical Property:

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Technology Process of phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester

There total 1 articles about phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

phenyl isocyanate (103-71-9) + 4,6-dimethyl-2-meraptopyrimidine (22325-27-5,131321-42-1) → phenylthiocarbamic acid S-4,6-dimethylpyrimidin-2-yl ester (1261073-47-5)

Guidance literature:

With [(Me3Si)2N]3Pr(μ-Cl)Li(THF)3; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/om100671s

upstream raw materials:

phenyl isocyanate

4,6-dimethyl-2-meraptopyrimidine