(3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Base Information

• Chemical Name: (3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione
• CAS No.: 169532-37-0
• Molecular Formula: C₂₇H₃₄Cl₂N₂O₄
• Molecular Weight: 521.484

Synonyms:(3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Chemical Property of (3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Chemical Property:

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Technology Process of (3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

There total 1 articles about (3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-{[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-butyric acid 3-((S)-2-{[1-(4-chloro-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-butyryloxy)-propyl ester (144406-59-7) → (3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (169532-37-0) + (3S,5R,6S,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (144489-91-8)

Guidance literature:

With methanesulfonic acid; zinc; In tetrahydrofuran; at 0 ℃; for 3h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)61145-0

Reference yield:

(3S,5R,6R,8S)-5,6-Bis-(4-chloro-phenyl)-3,8-diisopropyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (169532-37-0) → (1R,2R)-1,2-bis(4-chlorophenyl)ethane-1,2-diamine (822519-90-4)

Guidance literature:

With lead(IV) acetate; sodium hydroxide; Multistep reaction; 1) aq. EtOH, 2) H₂O;

DOI:10.1016/S0040-4039(00)61145-0

upstream raw materials:

(S)-2-{[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-butyric acid 3-((S)-2-{[1-(4-chloro-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-butyryloxy)-propyl ester

Downstream raw materials:

(1R,2R)-1,2-bis(4-chlorophenyl)ethane-1,2-diamine

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