3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

Base Information

Chemical Name:3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol
CAS No.:1352408-18-4
Molecular Formula:C₈₅H₁₂₇NO₁₀
Molecular Weight:1322.94
Hs Code.:

Synonyms:3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

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Chemical Property of 3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

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Technology Process of 3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

There total 1 articles about 3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1056024-93-1
(2S,3S,4R)-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-2-hexacosylaminooctadecane-1,3,4-triol

: 1352408-18-4
3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; water; at 20 ℃;
DOI:10.1039/c1ob06235b

Reference yield: 87.0%

: 1352408-18-4
3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

: 62-53-3
aniline

: (2S,3S,4R)-(2,3,4-tri-O-benzyl-N-phenyl-α-D-galactopyranuronamidyl)-3,4-di-O-benzyl-2-(hexacosanamido)octadecane-3,4-diol

Guidance literature:: 3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol; With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); In dichloromethane; N,N-dimethyl-formamide; for 0.5h;

aniline; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2015.04.068

Reference yield:

: 1352408-18-4
3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol

: 102-49-8
3,4-dichlorobenzyl amine

: (2S,3S,4R)-(2,3,4-tri-O-benzyl-N-(3,4-dichlorobenzyl)-α-d-galactopyranuronamidyl)-3,4-di-O-benzyl-2-(hexacosanamido)octadecane-3,4-diol

Guidance literature:: 3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2-hexacosylaminooctadecane-1,3,4-triol; With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); In dichloromethane; N,N-dimethyl-formamide; for 0.5h;

3,4-dichlorobenzyl amine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2015.04.068