(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Base Information

Chemical Name:(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine
CAS No.:142636-08-6
Molecular Formula:C₃₃H₄₈NOP
Molecular Weight:505.724
Hs Code.:

Synonyms:(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Suppliers and Price of (4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

There total 4 articles about (4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 69803-59-4
3-(diphenylphosphinoyl)-1-propanal

: 142636-07-5
(4E,8E)-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

: 142636-08-6
(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Guidance literature:: With sodium cyanoborohydride; In methanol; for 1h; Ambient temperature;
DOI:10.1021/jm00094a020

Reference yield:

: 889-57-6
3-(diphenylphosphinoyl)-1-propanol

: 142636-08-6
(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / oxalyl chloride / CH₂Cl₂; dimethylsulfoxide / 1.) -40 deg C, 1 h, 2.) -20 deg C, 1 h

2: 70 percent / NaBH₃CN / methanol / 1 h / Ambient temperature

With oxalyl dichloride; sodium cyanoborohydride; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00094a020

Reference yield:

: 51860-45-8
3-hydroxypropyltriphenylphosphonium bromide

: 142636-08-6
(4E,8E)-N-<3-(diphenylphosphinoyl)propyl>-N-methyl-5,9,13-trimethyl-4,8,12-tetradecatrienylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 50percent aq. NaOH / ethanol

2: 62 percent / oxalyl chloride / CH₂Cl₂; dimethylsulfoxide / 1.) -40 deg C, 1 h, 2.) -20 deg C, 1 h

3: 70 percent / NaBH₃CN / methanol / 1 h / Ambient temperature

With sodium hydroxide; oxalyl dichloride; sodium cyanoborohydride; In methanol; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00094a020