(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

Base Information

Chemical Name:(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine
CAS No.:1214738-02-9
Molecular Formula:C₃₂H₃₇NO₃
Molecular Weight:483.651
Hs Code.:

Synonyms:(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

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Chemical Property of (2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

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Technology Process of (2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

There total 3 articles about (2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (2R,3R,4R,5R)-2-allyl-3,4-bis(benzyloxy)-5-(benzyloxy-methyl)pyrrolidine

: 106-95-6
allyl bromide

: 1214738-02-9
(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.030

Reference yield:

: 158349-27-0
(3S,4R,5R)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)pyrrolidin-2-one

: 1214738-02-9
(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: Schwartz's reagent / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2: ytterbium(III) triflate / tetrahydrofuran / -25 - 20 °C / Inert atmosphere

3: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With Schwartz's reagent; tetra-(n-butyl)ammonium iodide; potassium carbonate; ytterbium(III) triflate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/d1ob01172c

Reference yield:

: 397242-80-7
(2R,3R,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-3,4-dihydro-2H-pyrrole

: 1214738-02-9
(2R,3R,4R,5R)-1,2-diallyl-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: ytterbium(III) triflate / tetrahydrofuran / -25 - 20 °C / Inert atmosphere

2: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; potassium carbonate; ytterbium(III) triflate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/d1ob01172c