1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene

Base Information

• Chemical Name: 1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene
• CAS No.: 1335044-17-1
• Molecular Formula: C₇₇H₃₀OSi
• Molecular Weight: 999.17

Synonyms:1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene

Chemical Property of 1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene

Chemical Property:

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Technology Process of 1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene

There total 1 articles about 1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C17H29ClMgOSi (1335044-16-0) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C60-Ih)[5,6]fullerene (1335044-17-1)

Guidance literature:

In tetrahydrofuran; N,N-dimethyl-formamide; 1,2-dichloro-benzene; at 25 ℃; for 1h;

DOI:10.1021/ja500340f

Reference yield: 98.0%

1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C60-Ih)[5,6]fullerene (1335044-17-1) → C154H58O2Si2 (1335044-18-2)

Guidance literature:

1-(dimethyl-o-2-ethylhexyloxyphenylsilylmethyl)-1,9-dihydro(C₆₀-I_h)[5,6]fullerene; With potassium tert-butylate; In tetrahydrofuran; 1,2-dichloro-benzene; at 25 ℃; for 0.75h;

With N-Bromosuccinimide; In tetrahydrofuran; 1,2-dichloro-benzene; at 25 ℃; for 2h;

DOI:10.1021/ja500340f

upstream raw materials:

C₁₇H₂₉ClMgOSi

fullerene-C₆₀

Downstream raw materials:

C₁₅₄H₅₈O₂Si₂

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