{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

Base Information

Chemical Name:{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid
CAS No.:1354765-95-9
Molecular Formula:C₁₉H₁₈F₃N₇O₇S₂
Molecular Weight:577.522
Hs Code.:

{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

Synonyms:{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

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Chemical Property of {1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

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Technology Process of {1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

There total 2 articles about {1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 900090-60-0
N-{5-({1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}sulfamoyl)-1,3,4-thiadiazol-2-yl}acetamide

: 1354765-95-9
{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

Guidance literature:: With hydrogenchloride; In water; for 1h; Reflux;
DOI:10.1007/s11172-012-0297-x

Reference yield:

: C₈H₇F₃N₄O₅S₂

: 1354765-95-9
{1-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trioxo-5-trifluoromethyl-2,3,4,5,6,7-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-5-yl}amide of 5-amino-1,3,4-thiadiazol-2-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 - 100 °C

2: hydrogenchloride / water / 1 h / Reflux

With hydrogenchloride; triethylamine; In water; N,N-dimethyl-formamide;
DOI:10.1007/s11172-012-0297-x