phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside
CAS No.:1227636-94-3
Molecular Formula:C₉₇H₁₁₈O₂₃SSi
Molecular Weight:1712.14
Hs Code.:

phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

Synonyms:phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

There total 2 articles about phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1227636-95-4
C₃₈H₅₀Cl₃NO₉Si

: 1227637-18-4
phenyl O-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

: 1227636-94-3
phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja1009037

Reference yield:

: 1227636-95-4
C₃₈H₅₀Cl₃NO₉Si

: 1227637-18-4
phenyl O-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

: C₉₇H₁₁₈O₂₃SSi

: 1227636-94-3
phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.0833333h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja1009037

Reference yield: 82.0%

: 1227636-94-3
phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-2-O-allyl-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

: 1227636-96-5
phenyl [6-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->2)-[3,4,6-tri-O-(p-methoxybenzyl)-α-D-mannopyranosyl]-(1->6)-3,4-di-O-(p-methoxybenzyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In tetrahydrofuran; hexane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja1009037