2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

Base Information

Chemical Name:2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride
CAS No.:949006-08-0
Molecular Formula:C₃₀H₃₂FN₃O₈
Molecular Weight:581.598
Hs Code.:

Synonyms:2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

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Chemical Property of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

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Technology Process of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

There total 2 articles about 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 949006-05-7
2-azido-3,6-di-O-benzyl-2-deoxy-β-D-galactopyranosyl fluoride

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 949006-08-0
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

Guidance literature:: With dmap; In pyridine; at 20 - 50 ℃; for 5h;
DOI:10.1016/j.tet.2007.05.126

Reference yield:

: C₂₃H₂₁O₅N₃F₆

: 949006-08-0
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine; ethanol / 55.5 h / 20 °C

2: 69 percent / DMAP / pyridine / 5 h / 20 - 50 °C

With dmap; In pyridine; ethanol;
DOI:10.1016/j.tet.2007.05.126

Reference yield:

: 949006-08-0
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,5-trimethoxybenzoyl)-β-D-galactopyranosyl fluoride

: C₄₂H₄₉O₇N₉Si

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / AgClO₄; Cp₂HfCl₂; 4 Angstroem molecular sieves / toluene / 42 h / 20 °C

2: 43 percent / NaOMe / methanol / 50 °C

With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; sodium methylate; silver perchlorate; In methanol; toluene;
DOI:10.1016/j.tet.2007.05.126