Technology Process of 3,7-bis(9,9-di-n-hexylfluoren-2-yl)-N-(4-n-butylphenyl)phenothiazine-S,S-dioxide
There total 5 articles about 3,7-bis(9,9-di-n-hexylfluoren-2-yl)-N-(4-n-butylphenyl)phenothiazine-S,S-dioxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate;
In
1,4-dioxane; water; toluene;
at 90 ℃;
for 16h;
Inert atmosphere;
DOI:10.1002/pola.24527
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tris-(dibenzylideneacetone)dipalladium(0); tri-tertiary-butyl phosphonium tetrafluoroborate / toluene
2: N-Bromosuccinimide / dichloromethane
3: dihydrogen peroxide / acetic acid
4: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate / 1,4-dioxane; water; toluene / 16 h / 90 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); N-Bromosuccinimide; tri-tertiary-butyl phosphonium tetrafluoroborate; dihydrogen peroxide;
In
1,4-dioxane; dichloromethane; water; acetic acid; toluene;
4: Suzuki-Miyaura coupling;
DOI:10.1002/pola.24527
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dihydrogen peroxide / acetic acid
2: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate / 1,4-dioxane; water; toluene / 16 h / 90 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; dihydrogen peroxide;
In
1,4-dioxane; water; acetic acid; toluene;
2: Suzuki-Miyaura coupling;
DOI:10.1002/pola.24527
