2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

Base Information

Chemical Name:2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride
CAS No.:61984-13-2
Molecular Formula:C₁₁H₉Cl₃N₂O₅S
Molecular Weight:387.628
Hs Code.:

Synonyms:2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

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Chemical Property of 2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

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Technology Process of 2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

There total 1 articles about 2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61561-24-8
2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetic acid

: 61984-13-2
2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

Guidance literature:: With phosphorus pentachloride; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1021/jm00133a018

Reference yield: 87.0%

: 66429-65-0
(6R)-7t-amino-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-(6rH)-5-oxa-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

: 61984-13-2
2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

: 75819-43-1
(6R,7S)-7-[2-[(Z)-Hydroxyimino]-2-(4-methanesulfonylamino-phenyl)-acetylamino]-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-5-oxa-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.833333h;
DOI:10.1021/jm00133a018

Reference yield:

: 61984-13-2
2-<4-(mesylamino)phenyl>-2-(Z)-<(dichloroacetoxy)imino>acetyl chloride

: 75670-09-6
(6R,7S)-7-[2-[(Z)-Hydroxyimino]-2-(4-methanesulfonylamino-phenyl)-acetylamino]-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-5-oxa-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / CH₂Cl₂ / 0.83 h / 0 °C

2: 100 percent / anisole, TFA / CH₂Cl₂ / 0.83 h

With pyridine; methoxybenzene; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00133a018