{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

Base Information

Chemical Name:{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron
CAS No.:126670-40-4
Molecular Formula:C₁₇H₁₂FeO₃
Molecular Weight:320.127
Hs Code.:

Synonyms:{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

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Chemical Property of {5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

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Technology Process of {5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

There total 1 articles about {5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: tricarbonyl(cyclohexadienyl)iron tetrafluoroborate

: 1007-47-2
(phenylethynyl)dimethylaluminum

: 126670-40-4
{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

Guidance literature:: In diethyl ether; molar ratio 2.2/1.0, stirring at 0°C, reaction time 1 h 45 min; mixture poured into a satd. solution of KH2PO4, add drops H2SO4, layers separated, organic layer washed with NaHCO3 and NaCl solution and dried, removal of the solvent, chromy. (silica gel, 10% ether in hexane), NMR, IR, mass spectra;
DOI:10.1016/0022-328X(89)85123-X

Reference yield: 94.0%

: ceric(IV) ammonium nitrate

: 126670-40-4
{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

: 5-(2-phenylethynyl)cyclohexa-1,3-diene

Guidance literature:: With triethylamine; In acetone; at 0°C; purification by chromy.;
DOI:10.1016/0022-328X(89)85123-X

Reference yield:

: 126670-40-4
{5-(2'-phenylethynyl)cyclohexadiene}tricarbonyliron

: cis-C₆H₇Fe(CO)3CHCHC₆H₅

Guidance literature:: With hydrogen; In ethanol; hydrogenation in absolute ethanol at H2 pressure of 1 atm; NMR, mass spectra;
DOI:10.1016/0022-328X(89)85123-X