(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

Base Information

Chemical Name:(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester
CAS No.:169956-62-1
Molecular Formula:C₁₇H₁₇N₅O₂S₃
Molecular Weight:419.552
Hs Code.:

(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid <i>S</i>-benzothiazol-2-yl ester

Synonyms:(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

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Chemical Property of (5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

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Technology Process of (5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

There total 4 articles about (5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 120-78-5
di(benzothiazol-2-yl)disulfide

: 114768-90-0
(5-Amino-[1,2,4]thiadiazol-3-yl)-[(Z)-cyclohexyloxyimino]-acetic acid

: 169956-62-1
(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

Guidance literature:: With tributyl-amine; triethyl phosphite; In acetonitrile; at -10 ℃;
DOI:10.7164/antibiotics.53.1071

Reference yield:

: 108-85-0
1-bromocyclohexane

: 169956-62-1
(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 67 percent / potassium carbonate; 18-crown-6 / dimethylsulfoxide

2.1: NH₂NH₂*H₂O / CH₂Cl₂; methanol / 20 °C

2.2: 99 percent / HCl / ethanol

3.1: 28 percent / NaOH / H₂O / 20 °C / pH 5.0

4.1: 60 percent / P(OEt)3; tri-n-butylamine / acetonitrile / -10 °C

With sodium hydroxide; 18-crown-6 ether; tributyl-amine; potassium carbonate; hydrazine hydrate; triethyl phosphite; In methanol; dichloromethane; water; dimethyl sulfoxide; acetonitrile;
DOI:10.7164/antibiotics.53.1071

Reference yield:

: 54488-64-1
O-cyclohexylhydroxylamine hydrochloride

: 169956-62-1
(5-amino-[1,2,4]thiadiazol-3-yl)-cyclohexyloxyimino-thioacetic acid S-benzothiazol-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / NaOH / H₂O / 20 °C / pH 5.0

2: 60 percent / P(OEt)3; tri-n-butylamine / acetonitrile / -10 °C

With sodium hydroxide; tributyl-amine; triethyl phosphite; In water; acetonitrile;
DOI:10.7164/antibiotics.53.1071