2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

Base Information

Chemical Name:2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine
CAS No.:1415328-13-0
Molecular Formula:C₂₁H₂₄FN₃O₃
Molecular Weight:385.438
Hs Code.:

Synonyms:2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

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Chemical Property of 2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

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Technology Process of 2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

There total 5 articles about 2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1071476-71-5
2-[2-(2-fluoroethoxy)ethoxy]ethyl 4-methylbenzene-1-sulfonate

: 1415328-11-8
4-(6-(methylamino)quinoxalin-2-yl)phenol

: 1415328-13-0
2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

Guidance literature:: In N,N-dimethyl-formamide; for 2h; Reflux;
DOI:10.1016/j.ejmech.2012.08.031

Reference yield:

: C₁₅H₁₁N₃O

: 1415328-13-0
2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Reflux

2: N,N-dimethyl-formamide / 2 h / Reflux

With sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.031

Reference yield:

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 1415328-13-0
2-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)phenyl)-N-methylquinoxalin-6-amine

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / 20 °C

2: hydrazine hydrate; palladium on activated charcoal / ethanol / Reflux

3: sodium methylate / methanol / 2 h / Reflux

4: sodium tetrahydroborate / methanol / 1 h / 0 °C / Reflux

5: N,N-dimethyl-formamide / 2 h / Reflux

With sodium tetrahydroborate; palladium on activated charcoal; sodium methylate; hydrazine hydrate; In methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.031