3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1346235-81-1
Molecular Formula:C₂₉H₂₃BF₂N₂O₃
Molecular Weight:496.321
Hs Code.:

Synonyms:3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.5%

: 277313-50-5
7-hydroxy-2-oxo-2H-chromene-3-carbaldehyde

: phenyl BODIPY

: 1346235-81-1
3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With piperidine; acetic acid; In toluene; Reflux; Inert atmosphere;
DOI:10.1021/ol202595t

Reference yield: 95.7%

: 13154-24-0
triisopropylsilyl chloride

: 1346235-81-1
3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

: 1346235-82-2
3-(2-(7-triisopropylsilyloxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 3-(2-(7-hydroxy-2-oxo-2H-chromene-3-yl)ethenyl)-4,4-difluoro-8-phenyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene; With dmap; triethylamine; In dichloromethane; for 0.166667h; Cooling with ice;

triisopropylsilyl chloride; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/ol202595t