(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

Base Information

Chemical Name:(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol
CAS No.:1216934-98-3
Molecular Formula:C₂₁H₂₅F₂N₃O₅
Molecular Weight:437.443
Hs Code.:

Synonyms:(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

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Chemical Property of (2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

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Technology Process of (2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

There total 1 articles about (2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1216934-96-1
(4S,6R)-4-[(1S)-1-azido-2-(3,5-difluoro-phenoxy)-ethyl]-6-methoxy-2-(4-methoxy-phenyl)-[1,3]dioxepane

: 1216934-97-2
(2S,3S,5R)-2-azido-1-(3,5-difluoro-phenoxy)-5-methoxy-6-(4-methoxy-benzyloxy)-hexan-3-ol

: 1216934-98-3
(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

Guidance literature:: With chloro-trimethyl-silane; sodium cyanoborohydride; In acetonitrile; at 0 ℃; Molecular sieve;

Reference yield: 63.0%

: 1216934-98-3
(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

: 108-95-2,27073-41-2
phenol

: 1216934-99-4
(2S,3S,5R)-2-azido-1-(3,5-difluoro-phenoxy)-3-(4-methoxybenzyloxy)-5-methoxy-6-phenoxy-hexane

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.ejmech.2009.10.041

Reference yield: 61.0%

: 1216934-98-3
(2R,4S,5S)-5-azido-6-(3,5-difluoro-phenoxy)-2-methoxy-4-(4-methoxy-benzyloxy)-hexan-1-ol

: 42060-32-2
N-benzyl-2-nitrobenzenesulfonamide

: 1216935-03-3
N-[5-(5S)-azido-6-(3,5-difluoro-phenoxy)-2-(2R)-methoxy-4-(4S)-(4-methoxy-benzyloxy)-hexyl]-N-benzyl-2-nitro-benzenesulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2009.10.041