12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

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Chemical Name:12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone
CAS No.:93832-95-2
Molecular Formula:C₃₁H₃₄N₆O₄
Molecular Weight:554.649
Hs Code.:

Synonyms:12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

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Chemical Property of 12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

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Technology Process of 12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

There total 3 articles about 12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 93832-89-4
10-Butyl-8-butylamino-3-methyl-5,10-dihydro-1H-pyrimido[4,5-b]quinoline-2,4-dione

: 35824-99-8
3-phenyl-5-formyl-6-chlorouracil

: 93832-95-2
12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

Guidance literature:: In chloroform; for 3h; Heating;
DOI:10.1039/c39840000872

Reference yield:

: 93832-84-9
10-Butyl-8-butylamino-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

: 93832-95-2
12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol / Heating

2: 43 percent / CHCl₃ / 3 h / Heating

With sodium tetrahydroborate; In ethanol; chloroform;
DOI:10.1039/c39840000872

Reference yield:

: 93832-80-5
10-Butyl-8-chloro-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

: 93832-95-2
12,14-Dibutyl-3-methyl-9-phenyl-5,7,12,14-tetrahydro-1H,11H-1,3,9,11,12,14-hexaaza-pentacene-2,4,8,10-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / hexamethylphosphoric acid triamide / 5 h / 100 °C

2: NaBH₄ / ethanol / Heating

3: 43 percent / CHCl₃ / 3 h / Heating

With sodium tetrahydroborate; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; chloroform;
DOI:10.1039/c39840000872