1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

Base Information

Chemical Name:1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide
CAS No.:1354932-51-6
Molecular Formula:C₂₂H₂₆IN₂*I
Molecular Weight:572.271
Hs Code.:

Synonyms:1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

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Chemical Property of 1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

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Technology Process of 1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

There total 4 articles about 1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 930102-07-1
1-butyl-5-iodo-2,3,3-trimethyl-3H-indol-1-ium iodide

: 864131-95-3
N,N'-diphenylformamidine

: 1354932-51-6
1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

Guidance literature:: With orthoformic acid triethyl ester; In ethanol; for 6h; Reflux;
DOI:10.1016/j.tet.2011.11.041

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1354932-51-6
1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / acetonitrile / 4 h / Reflux

2: acetonitrile / 24 h / Reflux

3: orthoformic acid triethyl ester / ethanol / 6 h / Reflux

With acetic acid; orthoformic acid triethyl ester; In ethanol; acetonitrile;
DOI:10.1016/j.tet.2011.11.041

Reference yield:

: 54136-25-3
5-iodo-2,3,3-trimethyl-3H-indole

: 1354932-51-6
1-butyl-5-iodo-3,3-dimethyl-2-[(E)-2-(phenylamino)ethenyl]-3H-indolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 24 h / Reflux

2: orthoformic acid triethyl ester / ethanol / 6 h / Reflux

With orthoformic acid triethyl ester; In ethanol; acetonitrile;
DOI:10.1016/j.tet.2011.11.041