(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

Base Information

Chemical Name:(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone
CAS No.:810676-41-6
Molecular Formula:C₁₅H₁₇IO
Molecular Weight:340.204
Hs Code.:

Synonyms:(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

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Technology Process of (Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

There total 2 articles about (Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 72946-37-3
1-hydroxy-1-(2-phenylethynyl)cycloheptane

: 810676-41-6
(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

Guidance literature:: With poly[styrene(iodosodiacetate)]; iodine; In dichloromethane; at 20 ℃; for 11h;
DOI:10.1055/s-2004-831214

Reference yield:

: 536-74-3
phenylacetylene

: 810676-41-6
(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg; I₂; EtBr / tetrahydrofuran / 1 h / 20 °C

1.2: tetrahydrofuran / 2 h / 0 °C

2.1: 67 percent / poly[styrene(iodosodiacetate)]; I₂ / CH₂Cl₂ / 11 h / 20 °C

With poly[styrene(iodosodiacetate)]; iodine; ethidium Bromide; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2004-831214

Reference yield: 92.0%

: 536-74-3
phenylacetylene

: 810676-41-6
(Z)-2-(1-iodo-1-phenyl)methylenecyclooctanone

: (Z)-2-(1-phenyl-1-phenylethynyl)methylenecyclooctanone

Guidance literature:: With copper(l) iodide; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In acetonitrile; at 60 ℃; for 12h;
DOI:10.1055/s-2004-831214