trans-3,5-dichlorocinnamic acid tert-butyl ester

Base Information

Chemical Name:trans-3,5-dichlorocinnamic acid tert-butyl ester
CAS No.:230642-77-0
Molecular Formula:C₁₃H₁₄Cl₂O₂
Molecular Weight:273.159
Hs Code.:

Synonyms:trans-3,5-dichlorocinnamic acid tert-butyl ester

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Chemical Property of trans-3,5-dichlorocinnamic acid tert-butyl ester

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Technology Process of trans-3,5-dichlorocinnamic acid tert-butyl ester

There total 2 articles about trans-3,5-dichlorocinnamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 39943-56-1
3,5-dichlorophenylhydrazine

: 230642-77-0
trans-3,5-dichlorocinnamic acid tert-butyl ester

Guidance literature:: With Bathocuproine; palladium diacetate; acetic acid; In methanol; chlorobenzene; at 40 ℃; for 3h; under 760.051 Torr; chemoselective reaction;
DOI:10.1021/ol202862t

Reference yield: 77.0%

: 10203-08-4
3,5-dichlorobenzaldehyde

: 27784-76-5
tert-butyl diethylphosphonoacetate

: 230642-77-0
trans-3,5-dichlorocinnamic acid tert-butyl ester

Guidance literature:: tert-butyl diethylphosphonoacetate; With sodium hexamethyldisilazane; In tetrahydrofuran; toluene; at 25 ℃; for 0.5h;

3,5-dichlorobenzaldehyde; In tetrahydrofuran; toluene; at 20 ℃; Further stages.;
DOI:10.1021/jm010100v

Reference yield:

: 24470-78-8
isopropyltriphenylphosphonium iodide

: 230642-77-0
trans-3,5-dichlorocinnamic acid tert-butyl ester

: (1S,3R)-3-(3,5-Dichloro-phenyl)-2,2-dimethyl-cyclopropanecarboxylic acid tert-butyl ester

Guidance literature:: isopropyltriphenylphosphonium iodide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

trans-3,5-dichlorocinnamic acid tert-butyl ester; In tetrahydrofuran; hexane; at 0 - 25 ℃; Further stages.;
DOI:10.1021/jm010100v