(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

Base Information

Chemical Name:(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester
CAS No.:204197-15-9
Molecular Formula:C₁₆H₁₁F₅N₄O₆
Molecular Weight:450.279
Hs Code.:

Synonyms:(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

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Chemical Property of (2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

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Technology Process of (2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

There total 3 articles about (2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 14533-84-7
pentafluorophenyl trifloroacetate

: 204197-14-8
(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester

: 204197-15-9
(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 23 ℃; for 24h;

Reference yield:

: 152178-79-5
5-acetamido-2,6-anhydro-4-azido-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

: 204197-15-9
(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaIO₄ / methanol / 0.5 h / 23 °C

2: NaClO₂, aq. KH₂PO₄, cyclohexene / 2-methyl-propan-2-ol / 3 h / 23 °C

3: 47 percent / pyridine / dimethylformamide / 24 h / 23 °C

With pyridine; sodium chlorite; sodium periodate; potassium dihydrogenphosphate; cyclohexene; In methanol; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: methyl 5-acetamido-4-azido-2,6-anhydro-3,4,5-trideoxy-6-formyl-L-gluco-hex-2-enonate

: 204197-15-9
(2R,3R,4S)-3-Acetylamino-4-azido-3,4-dihydro-2H-pyran-2,6-dicarboxylic acid 6-methyl ester 2-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaClO₂, aq. KH₂PO₄, cyclohexene / 2-methyl-propan-2-ol / 3 h / 23 °C

2: 47 percent / pyridine / dimethylformamide / 24 h / 23 °C

With pyridine; sodium chlorite; potassium dihydrogenphosphate; cyclohexene; In N,N-dimethyl-formamide; tert-butyl alcohol;